![](/CAS/GIF/865-50-9.gif)
IODOMETHANE-D3 synthesis
- Product Name:IODOMETHANE-D3
- CAS Number:865-50-9
- Molecular formula:CD3I
- Molecular Weight:144.96
![Methanol-d4](/CAS/GIF/811-98-3.gif)
811-98-3
199 suppliers
$18.69/1g
![IODOMETHANE-D3](/CAS/GIF/865-50-9.gif)
865-50-9
136 suppliers
$25.00/1g
Yield:865-50-9 83.8%
Reaction Conditions:
with hydrogen iodide in water at 40 - 50; for 4 h;
Steps:
3 Example 3: CD3- iodomethane (Compound 5A) Synthesis
To the reaction flask was added 5mL deuterated methanol, water and 50mL 5mL percentage of hydriodic acid (mass55.0% -58.0%, by mass percentage, means the mass of hydrogen iodide accounts for the total mass percentage hydroiodicStabilizer mass% hypophosphorous acid containing 1.5%, by mass percentage, means hypophosphorous acid; division ratioStabilizer mass percentage of the total mass of hydroiodic acid reagent), followed by stirring, the reaction was heated to 40 2h,The reaction was heated to 50 deg.] C 2h, cooled to room temperature (about 20 deg.] C), into a distillation apparatus, atmospheric pressure (1 atm for),40 ~ 45 collected fractions, the distillation rate of 0.1mL / second to give 13.25 g of a colorless liquid, yield 83.8%.
References:
Shanghai Institute of Organic Chemistry;Ding, Wenhui;Long, Qin;Li, Xiaoqiang;Fang, Tong;Yang, Jun CN104557815, 2016, B Location in patent:Paragraph 0105; 0106; 0107
![METHANOL-D3](/CAS/GIF/1849-29-2.gif)
1849-29-2
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$20.00/1ml
![IODOMETHANE-D3](/CAS/GIF/865-50-9.gif)
865-50-9
136 suppliers
$25.00/1g
![METHYL-D3 P-TOLUENESULFONATE](/CAS/GIF/7575-93-1.gif)
7575-93-1
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![IODOMETHANE-D3](/CAS/GIF/865-50-9.gif)
865-50-9
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$25.00/1g
![BROMOMETHANE-D3](/CAS/GIF/1111-88-2.gif)
1111-88-2
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$305.00/10g-eu
![IODOMETHANE-D3](/CAS/GIF/865-50-9.gif)
865-50-9
136 suppliers
$25.00/1g
![methyl-d3 radical](/CAS/20200119/GIF/2122-44-3.gif)
2122-44-3
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![IODOMETHANE-D3](/CAS/GIF/865-50-9.gif)
865-50-9
136 suppliers
$25.00/1g