IPI-9119 synthesis
- Product Name:IPI-9119
- CAS Number:1346564-56-4
- Molecular formula:C24H19F2N5O5
- Molecular Weight:495.43
811788-85-9
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Yield:-
Steps:
Multi-step reaction with 5 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 24 h
2.1: sulfuric acid; iron / ethanol; water; tetrahydrofuran / 1 h / 0 - 20 °C
3.1: sodium tetrahydroborate; acetic acid / 1 h / 20 °C
4.1: triethylamine / dichloromethane / 0.25 h / 0 - 20 °C
4.2: 3 h / Reflux
5.1: hydrogen / palladium 10% on activated carbon / ethyl acetate; methanol / 0.5 h / 20 °C
References:
US2011/274655,2011,A1
403-21-4
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1346567-63-2
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1346564-56-4
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![benzyl 3-phenoxy-4-[(propan-2-yl)amino]benzoate](/CAS/20200401/GIF/1346567-64-3.gif)