Isobutylene oxide synthesis
- Product Name:Isobutylene oxide
- CAS Number:558-30-5
- Molecular formula:C4H8O
- Molecular Weight:72.11
115-11-7
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558-30-5
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Yield:558-30-5 90%
Reaction Conditions:
with tert.-butylhydroperoxide;molybdenum(V) chloride in 1,2-dimethoxyethane at 120; under 3750.38 Torr; for 4 h;Inert atmosphere;Reagent/catalyst;Temperature;Solvent;Pressure;
Steps:
1.1; 2.1; 3.1 Preparation of epoxy isobutane
Add 150g isobutene, 1g MoCl5, 5g ethylene glycol, 300g tert-butyl hydroperoxide (TBHP) to a pressurized reaction kettle, charge N2 to a pressure of 0.5Mpa, at 120 Reaction 4h. The yield of the product epoxy isobutane (IBO) is 90%. 172 g of epoxy isobutane with a purity of 99.5% was obtained by distillation and separation
References:
CN108047013,2020,B Location in patent:Paragraph 0033; 0035; 0038; 0040; 0043; 0045
558-42-9
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558-30-5
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123-72-8
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78-84-2
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115-11-7
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558-30-5
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75-91-2
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115-11-7
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558-30-5
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75-65-0
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558-30-5
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85-01-8
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29526-99-6
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78-93-3
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