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ChemicalBook CAS DataBase List JHELVJNRWQYMIA-SECBINFHSA-N
1268729-59-4

JHELVJNRWQYMIA-SECBINFHSA-N synthesis

1synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: sodium hydride / tetrahydrofuran / 24 h / 20 °C
2: diazomethane / diethyl ether / 0 °C / Inert atmosphere

References:

Wang, San-Yong;Xu, Zhong-Liang;Wang, Hui;Li, Chun-Rong;Fu, Li-Wu;Pang, Ji-Yan;Li, Jing;She, Zhi-Gang;Lin, Yong-Cheng [Helvetica Chimica Acta,2012,vol. 95,# 6,p. 973 - 982]