Lepidine, 2,8-dichloro- (4CI) synthesis

5synthesis methods

Product Name:Lepidine, 2,8-dichloro- (4CI)
CAS Number:815583-95-0
Molecular formula:C10H7Cl2N
Molecular Weight:212.0753

634-47-9 Synthesis

634-47-9
160 suppliers
$41.00/5g

815583-95-0
25 suppliers
$21.00/250mg

Yield:-

Steps:

Multi-step reaction with 3 steps
1: nitric acid; concentrated sulfuric acid / 0 °C
2: Raney nickel; methanol; dioxane / Hydrogenation_.Die Einheitlichkeit des Praeparats ist nicht bewiesen
3: aqueous hydrochloric acid; sodium nitrite / Erwaermen der Rktlsg_. mit Kupfer(I)-chlorid und konz. wss. Salzsaeure

References:

Krahler;Burger [Journal of the American Chemical Society,1941,vol. 63,p. 2367,2370][Journal of the American Chemical Society,1942,vol. 64,p. 2417]

54904-38-0 Synthesis