LNEHHTWYEBGHBY-VWYCJHECSA-N synthesis
- Product Name:LNEHHTWYEBGHBY-VWYCJHECSA-N
- CAS Number:157967-06-1
- Molecular formula:C14H25NO5
- Molecular Weight:287.35
69610-40-8
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157967-06-1
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: 87 percent / SO3*pyridine, Et3N / dimethylsulfoxide / 2.5 h / 7 - 8 °C
2: 1.) i-Pr2N, n-BuLi, MgBr2*Et2O / 1.) THF, hexane, -78 deg C, 30 min; -78 deg C to r.t., 2 h; -78 deg C, 1 h, 2.) THF, -95 deg C, 2 h
3: 72 percent / proton sponge / CH2Cl2 / 36 h / Ambient temperature
4: 86 percent / H2 / 10percent Pd/C / methanol / 15 h / Ambient temperature
References:
Pettit, George R.;Singh, Sheo Bux;Herald, Delbert L.;Lloyd-Williams, Paul;Kantoci, Darko;et al. [Journal of Organic Chemistry,1994,vol. 59,# 21,p. 6287 - 6295]
158111-36-5
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157967-06-1
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15761-39-4
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$5.00/10g
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24424-99-5
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$13.50/25G
157967-06-1
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69610-41-9
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$9.00/1g
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