![](/CAS/20180808/GIF/33983-39-0.gif)
(+)-Medicarpin synthesis
- Product Name:(+)-Medicarpin
- CAS Number:33983-39-0
- Molecular formula:C16H14O4
- Molecular Weight:270.28
![2,4-Dimethoxyphenylacetic acid](/CAS/GIF/6496-89-5.gif)
6496-89-5
181 suppliers
$13.00/1g
![MEDICARPIN](/CAS/GIF/32383-76-9.gif)
32383-76-9
77 suppliers
$195.00/1 mg
![(+)-Medicarpin](/CAS/20180808/GIF/33983-39-0.gif)
33983-39-0
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: boron trifluoride diethyl etherate / 2 h / 90 - 100 °C
1.2: 50 - 90 °C
2.1: aluminum (III) chloride / acetonitrile / 0 °C / Reflux
2.2: Cooling with ice
3.1: sodium tetrahydroborate / ethanol / 0 - 20 °C
4.1: Lux cellulose-1 PHENOMENIX column / acetonitrile; water / Resolution of racemate
References:
Goel, Atul;Kumar, Amit;Hemberger, Yasmin;Raghuvanshi, Ashutosh;Jeet, Ram;Tiwari, Govind;Knauer, Michael;Kureel, Jyoti;Singh, Anuj K.;Gautam, Abnish;Trivedi, Ritu;Singh, Divya;Bringmann, Gerhard [Organic and Biomolecular Chemistry,2012,vol. 10,# 48,p. 9583 - 9592]
![Resorcinol](/CAS/GIF/108-46-3.gif)
108-46-3
747 suppliers
$10.00/10g
![MEDICARPIN](/CAS/GIF/32383-76-9.gif)
32383-76-9
77 suppliers
$195.00/1 mg
![(+)-Medicarpin](/CAS/20180808/GIF/33983-39-0.gif)
33983-39-0
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![4-BENZYLOXY-2-HYDROXYBENZALDEHYDE](/CAS/GIF/52085-14-0.gif)
52085-14-0
85 suppliers
$7.00/100mg
![(+)-Medicarpin](/CAS/20180808/GIF/33983-39-0.gif)
33983-39-0
56 suppliers
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