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ChemicalBook CAS DataBase List meso-Tetra(3-methylphenyl) porphine

meso-Tetra(3-methylphenyl) porphine synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 97 percent / MgBr2*OEt2; Et3N / CH2Cl2 / 60 °C
2: 81 percent / N-bromoacetamide / CHCl3 / 0.25 h / 0 - 20 °C
3: Na2CO3 / Pd(Ph3P)4 / toluene; methanol / 20 h / 70 °C
4: aq. HCl

References:

Shi, Dong-Fang;Wheelhouse, Richard T. [Tetrahedron Letters,2002,vol. 43,# 51,p. 9341 - 9342]

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