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1066-64-4

methanetetrayltetrakis[trimethylsilane] synthesis

13synthesis methods
-

Yield:1066-64-4 82%

Reaction Conditions:

Stage #1: (dichloromethyl)methylbis(trimethylsilyl)silane;methyllithium in diethyl ether at 20; for 12 h;
Stage #2: chloro-trimethyl-silane at 20; for 12 h;

References:

Schmohl, Kathleen;Reinke, Helmut;Oehme, Hartmut [European Journal of Inorganic Chemistry,2001,# 2,p. 481 - 489]