Methanone, (5-amino-2-methoxyphenyl)phenyl- synthesis

Yield:62261-53-4 66%

Reaction Conditions:

Stage #1: ortho-methoxybenzophenonewith pyridine;trifluorormethanesulfonic acid;lithium perchlorate in acetonitrile at 25;Electrochemical reaction;
Stage #2: with piperidine in acetonitrile at 80; for 12 h;Electrochemical reaction;

References:

Morofuji, Tatsuya;Shimizu, Akihiro;Yoshida, Jun-Ichi [Journal of the American Chemical Society,2013,vol. 135,# 13,p. 5000 - 5003] Location in patent:supporting information