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ChemicalBook CAS DataBase List METHIOTHEPIN MALEATE

METHIOTHEPIN MALEATE synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 78 percent Turnov. / 4-toluenesulfonic acid / 180 - 190 °C / 1) 1 h, atmospheric pressure; 2) 3 h in vacuo
2: 82 percent / Zn / acetic acid / 2 h / Heating

References:

Jilek;Pomykacek;Dlabac;et al. [Collection of Czechoslovak Chemical Communications,1980,vol. 45,# 2,p. 504 - 516]