METHYL 15-HYDROXYPENTADECANOATE synthesis
- Product Name:METHYL 15-HYDROXYPENTADECANOATE
- CAS Number:76529-42-5
- Molecular formula:C16H32O3
- Molecular Weight:272.42
67-56-1
739 suppliers
$7.29/5ml-f
106-02-5
241 suppliers
$20.00/1g
124-41-4
685 suppliers
$12.00/25g
76529-42-5
27 suppliers
$25.00/1mg
Yield:76529-42-5 98%
Reaction Conditions:
for 3 h;Heating / reflux;
Steps:
1
Methanol (150 mL) was added with 15-pentadecalactone (25.6 g), further added with 28% sodium methoxide solution (50 mL) and refluxed for 3 hours. The reaction solution was added with 1 N hydrochloric acid and extracted three times with ethyl acetate. The organic layer was washed with saturated brine and dried over anhydrous magnesium sulfate, and the solvent was removed to obtain methyl 15-hydroxypentadecanoate (28.5 g, yield: 98%).
References:
Fuji Photo Film Co. Ltd. EP1426353, 2004, A1 Location in patent:Page 14
67-56-1
739 suppliers
$7.29/5ml-f
106-02-5
241 suppliers
$20.00/1g
76529-42-5
27 suppliers
$25.00/1mg
106-02-5
241 suppliers
$20.00/1g
76529-42-5
27 suppliers
$25.00/1mg
1931-69-7
0 suppliers
inquiry
76529-42-5
27 suppliers
$25.00/1mg
