METHYL-2-BROMO-4-BROMOMETHYLBENZOATE synthesis
- Product Name:METHYL-2-BROMO-4-BROMOMETHYLBENZOATE
- CAS Number:128577-48-0
- Molecular formula:C9H8Br2O2
- Molecular Weight:307.97
87808-49-9
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$8.00/1g
128577-48-0
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$11.00/100mg
Yield: 94%
Reaction Conditions:
with tert.-butylhydroperoxide;cetyltrimethylammonim bromide;potassium bromide in water at 120; under 750.075 Torr;Microwave irradiation;
Steps:
General procedure: The reaction mixture was treated in a controlled microwavesynthesizer (Biotage Initiator+SP Wave model, 0-200 W at2.45 GHz, capped at 60 W during steady state) for severalminutes (the reaction attained 120 °C at 1 bar pressure). Thefinal products were isolated by column chromatographyusing an EtOAc-hexane gradient
References:
Reddy, Kancharla Rajendar;Rajanna, Kamatala C.;Venkateswarlu, Marri;Saiprakash [Synlett,2014,vol. 25,# 17,art. no. ST-2014-D0547-L,p. 2485 - 2487]
7697-27-0
204 suppliers
$6.00/1g
128577-48-0
114 suppliers
$11.00/100mg