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methyl 2-(methoxy(methyl)amino)-2-oxoacetate synthesis

1synthesis methods
5781-53-3 Synthesis
METHYL OXALYL CHLORIDE

5781-53-3
215 suppliers
$8.00/10g

6638-79-5 Synthesis
N,O-Dimethylhydroxylamine hydrochloride

6638-79-5
556 suppliers
$6.00/25g

methyl 2-(methoxy(methyl)amino)-2-oxoacetate

139507-50-9
3 suppliers
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Yield: 97%

Reaction Conditions:

with triethylamine in dichloromethane at 0 - 20; for 24 h;Inert atmosphere;

References:

Gediya, Shweta K.;Vyas, Vijyesh K.;Clarkson, Guy J.;Wills, Martin [Organic Letters,2021,vol. 23,# 20,p. 7803 - 7807] Location in patent:supporting information