ChemicalBook CAS DataBase List Methyl 3-(2-carboxyphenyl)benzoate

Methyl 3-(2-carboxyphenyl)benzoate synthesis

4synthesis methods

Product Name:Methyl 3-(2-carboxyphenyl)benzoate
CAS Number:171905-91-2
Molecular formula:C15H12O4
Molecular Weight:0

824-94-2 Synthesis

824-94-2
443 suppliers
$24.19/5G

171905-91-2
9 suppliers
$752.00/5g

Yield:-

Steps:

Multi-step reaction with 3 steps
1: potassium carbonate; tetra-(n-butyl)ammonium iodide / tetrahydrofuran / 6 h / Reflux
2: sodium carbonate; trans-bis(triphenylphosphine)palladium dichloride / tetrahydrofuran; water / 60 °C / Inert atmosphere
3: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

References:

Li, Yan;Ding, Yan-Jun;Wang, Jian-Yong;Su, Yi-Ming;Wang, Xi-Sheng [Organic Letters,2013,vol. 15,# 11,p. 2574 - 2577]

99769-19-4 Synthesis