Methyl 3-(3-hydroxyprop-1-yn-1-yl)benzoate synthesis
- Product Name:Methyl 3-(3-hydroxyprop-1-yn-1-yl)benzoate
- CAS Number:121114-45-2
- Molecular formula:C11H10O3
- Molecular Weight:190.2
618-91-7
138 suppliers
$11.00/5g
107-19-7
5 suppliers
$12.00/25g
121114-45-2
17 suppliers
$60.00/100mg
Yield:121114-45-2 99 %
Reaction Conditions:
Stage #1: methyl 3-iodo-benzoatewith bis-triphenylphosphine-palladium(II) chloride;copper(l) iodide;triethylamine at 20;Inert atmosphere;
Stage #2: propargyl alcohol at 20;Inert atmosphere;
References:
Lee, Seung Hoon;Chi, Hyung Min [Organic Letters,2023,vol. 25,# 7,p. 1083 - 1087] Location in patent:supporting information