Methyl 4-aMino-6-chloronicotinate synthesis
- Product Name:Methyl 4-aMino-6-chloronicotinate
- CAS Number:1256785-40-6
- Molecular formula:C7H7ClN2O2
- Molecular Weight:186.6
1830-54-2
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1256785-40-6
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$31.00/100mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: acetic anhydride; acetic acid / 1.5 h / 120 °C
1.2: 1 h / Cooling with ice
2.1: triethylamine; trichlorophosphate / 2 h / 0 - 120 °C
3.1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C
4.1: sulfuric acid / 0.25 h / 0 °C
4.2: pH 4 - 10
References:
Luk, Kin-Chun US2012/184562, 2012, A1
1374215-05-0
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1256785-40-6
59 suppliers
$31.00/100mg
79398-27-9
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$11.00/250mg
1256785-40-6
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$31.00/100mg
65973-52-6
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$6.00/1g
1256785-40-6
59 suppliers
$31.00/100mg