METHYL 4-CHLOROCUBANECARBOXYLATE synthesis

6synthesis methods

Product Name:METHYL 4-CHLOROCUBANECARBOXYLATE
CAS Number:122200-62-8
Molecular formula:C10H9ClO2
Molecular Weight:196.63

methyl 4-(chlorocarbonyl)cubane-1-carboxylate(WXG01537)

60462-18-2
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122200-62-8
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Yield:122200-62-8 500 mg

Reaction Conditions:

with dmap;2-mercaptopyridine-1-oxide sodium salt in tetrachloromethane; for 2 h;Irradiation;

References:

Chalmers, Benjamin A.;Xing, Hui;Houston, Sevan;Clark, Charlotte;Ghassabian, Sussan;Kuo, Andy;Cao, Benjamin;Reitsma, Andrea;Murray, Cody-Ellen P.;Stok, Jeanette E.;Boyle, Glen M.;Pierce, Carly J.;Littler, Stuart W.;Winkler, David A.;Bernhardt, Paul V.;Pasay, Cielo;De Voss, James J.;McCarthy, James;Parsons, Peter G.;Walter, Gimme H.;Smith, Maree T.;Cooper, Helen M.;Nilsson, Susan K.;Tsanaktsidis, John;Savage, G. Paul;Williams, Craig M. [Angewandte Chemie - International Edition,2016,vol. 55,# 11,p. 3580 - 3585][Angew. Chem.,2016,vol. 128,# 11,p. 3644 - 3649,6] Location in patent:supporting information