Methyl 5-fluoro-2-phenylbenzoate synthesis

4synthesis methods

Product Name:Methyl 5-fluoro-2-phenylbenzoate
CAS Number:1247810-91-8
Molecular formula:C14H11FO2
Molecular Weight:230.23

345-16-4 Synthesis

345-16-4
259 suppliers
$18.00/1g

1247810-91-8
11 suppliers
$265.00/250mg

Yield:-

Steps:

Multi-step reaction with 3 steps
1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere
2: triethylamine / dichloromethane / 12 h / -78 - 20 °C / Inert atmosphere
3: bis(triphenylphosphine)palladium(II) dichloride; sodium carbonate / tetrahydrofuran; water / 14 h / 80 °C / Schlenk technique; Inert atmosphere; Sealed tube

References:

Morack, Tobias;Metternich, Jan B.;Gilmour, Ryan [Organic Letters,2018,vol. 20,# 5,p. 1316 - 1319]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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98-80-6 Synthesis

98-80-6
718 suppliers
$5.00/5g

1247810-91-8
11 suppliers
$265.00/250mg

References

6942-39-8
115 suppliers
$34.00/5g

71-43-2
678 suppliers
$11.19/25ML

1247810-91-8
11 suppliers
$265.00/250mg

References

391-92-4
103 suppliers
$50.00/1g

1247810-91-8
11 suppliers
$265.00/250mg

References