Methyl 5-(tert-butyl)picolinate synthesis
- Product Name:Methyl 5-(tert-butyl)picolinate
- CAS Number:215436-29-6
- Molecular formula:C11H15NO2
- Molecular Weight:193.24
67-56-1
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120-80-9
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1465282-71-6
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215436-29-6
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Yield:1465282-71-6 59% ，215436-29-6 7%
Reaction Conditions:
Stage #1: methanol;benzene-1,2-diolwith pyridine;oxygen;1,4,7-triazacyclononane;iron(II) bromide for 16 h;Inert atmosphere;
Stage #2: with ammonium formate at 60; for 48 h;
References:
Guimond, Nicolas;Mayer, Peter;Trauner, Dirk [Chemistry - A European Journal,2014,vol. 20,# 31,p. 9519 - 9523] Location in patent:supporting information
67-56-1
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201230-82-2
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102236-19-1
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215436-29-6
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