![](/CAS/GIF/93-58-3.gif)
Methyl benzoate synthesis
- Product Name:Methyl benzoate
- CAS Number:93-58-3
- Molecular formula:C8H8O2
- Molecular Weight:136.15
![Methanol](/CAS/GIF/67-56-1.gif)
67-56-1
737 suppliers
$9.00/25ml
![Benzoic acid](/CAS/GIF/65-85-0.gif)
65-85-0
1332 suppliers
$10.00/25g
![Methyl benzoate](/CAS/GIF/93-58-3.gif)
93-58-3
468 suppliers
$14.00/25mL
Yield:93-58-3 100%
Reaction Conditions:
with 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione at 60; for 7 h;Reagent/catalyst;Temperature;
Steps:
1; 1-3; 2 Example 1: Preparation of methyl benzoate
Add 10mmol of benzoic acid, 100mmol of methanol, and 2mmol of dibromohydantoin into a 50mL three-necked flask, set up a reflux device, and stir for reaction at 60°C for 7h.After the methanol is recovered by rotary evaporation, it is transferred to a separatory funnel, and 20 mL of ethyl acetate is added, washed with 5% sodium carbonate solution, washed with water, dried with anhydrous sodium sulfate, and the solvent is removed under reduced pressure. The yield of methyl benzoate is 100%.
References:
CN113248373,2021,A Location in patent:Paragraph 0019; 0023-0032
![Methanol](/CAS/GIF/67-56-1.gif)
67-56-1
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![1-PHENYL-1-HEXANOL](/CAS/GIF/4471-05-0.gif)
4471-05-0
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$60.00/100mg
![Methyl benzoate](/CAS/GIF/93-58-3.gif)
93-58-3
468 suppliers
$14.00/25mL
![Methanol](/CAS/GIF/67-56-1.gif)
67-56-1
737 suppliers
$9.00/25ml
![BenzeneMethanol, alpha-(phenoxyMethyl)-](/CAS/GIF/4249-72-3.gif)
4249-72-3
58 suppliers
$9.00/250mg
![Methyl benzoate](/CAS/GIF/93-58-3.gif)
93-58-3
468 suppliers
$14.00/25mL