METHYL BRASSIDATE synthesis
- Product Name:METHYL BRASSIDATE
- CAS Number:7439-44-3
- Molecular formula:C23H44O2
- Molecular Weight:352.59
1679-53-4
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Yield:-
Steps:
Multi-step reaction with 5 steps
1: 75 percent / HBr, HOAc / a) r.t., 16 h, b) 100 deg C, 4 h
2: 90 percent / NaI / acetone / 16 h / Heating
3: 89 percent / 4 h / Ambient temperature
5: 1.) lithium hexamethyldisilazide, hexamethylphosphoramide / 1.) THF, 0 deg C, 10 min, 2.) THF, 0 deg C, 1 h
References:
Kling, Marcel R.;Easton, Christopher J.;Poulos, Alf [Journal of the Chemical Society. Perkin transactions I,1993,# 10,p. 1183 - 1190]
693-58-3
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50530-12-6
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1120-34-9
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