Molybdenum,bis(eta-benzene)- synthesis
- Product Name:Molybdenum,bis(eta-benzene)-
- CAS Number:12129-68-9
- Molecular formula:C12Mo
- Molecular Weight:240.08
Yield:12129-68-9 48%
Reaction Conditions:
with Al;AlCl3 in 1,3,5-trimethyl-benzene;(Schlenk) MoCl5, AlCl3, Al, mesitylene and benzene were refluxed for 76 h; all volatiles were removed in vac., the solid was broken up into small pieces and added to N2-satd. aq. soln. of KOH and N2S2O4 over 1 h at -20°C to -30°C, decanted, dried, extd. with boiling C6H6, evapd., washed with hexane, dried;
References:
Lund, Clinton L.;Schachner, Joerg A.;Quail, J. Wilson;Mueller, Jens [Journal of the American Chemical Society,2007,vol. 129,# 30,p. 9313 - 9320]
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