Monoallyl Phthalate synthesis
- Product Name:Monoallyl Phthalate
- CAS Number:3882-14-2
- Molecular formula:C11H10O4
- Molecular Weight:206.19
85-44-9
750 suppliers
$9.00/5g
107-18-6
2 suppliers
$24.60/100ml
3882-14-2
9 suppliers
$625.00/100mg
88-99-3
441 suppliers
$15.00/50g
Yield:3882-14-2 41% ，88-99-3 38%
Reaction Conditions:
for 1 h;Reflux;
Steps:
Alkoxycarbonyl Benzoic Acids 2a-g; General Procedure
General procedure: A solution of phthalic anhydride (1; 20.27 mmol) in the respective alcohol (10 mL) was stirred at reflux temperature until complete consumption of the starting material as determined by TLC analysis (1 h). Then, the solvent was evaporated under vacuo and the crude product was purified by silica gel column chromatography (EtOAc/hexane 3:7).
References:
Yassine, Hasna;Bouali, Jamila;Oumessaoud, Asmaa;Ourhzif, El Mahdi;Hamri, Salha;Hafid, Abderrafia;Khouili, Mostafa;Pujol, Maria Dolors [Synthesis,2021,vol. 53,# 11,p. 1971 - 1979]
85-44-9
750 suppliers
$9.00/5g
107-18-6
2 suppliers
$24.60/100ml
3882-14-2
9 suppliers
$625.00/100mg
182342-88-7
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3882-14-2
9 suppliers
$625.00/100mg