ChemicalBook CAS DataBase List Morpholine-3-carboxylic acid dimethylamide

Morpholine-3-carboxylic acid dimethylamide synthesis

3synthesis methods

Product Name:Morpholine-3-carboxylic acid dimethylamide
CAS Number:1101987-05-6
Molecular formula:C7H14N2O2
Molecular Weight:158.2

3-MORPHOLINECARBOXYLIC ACID METHYL ESTER

126264-49-1
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Morpholine-3-carboxylic acid dimethylamide

1101987-05-6
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: triethylamine / tetrahydrofuran / 20 °C
2: water; sodium hydroxide / methanol / 3 h / 75 °C
3: triethylamine; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; dmap / dichloromethane / 20 °C
4: trifluoroacetic acid / dichloromethane / 4 h / 20 °C

References:

WO2015/193506,2015,A1

MORPHOLINE-3,4-DICARBOXYLIC ACID 4-TERT-BUTYL ESTER 3-METHYL ESTER

212650-45-8
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References

212650-43-6 Synthesis

MORPHOLINE-3,4-DICARBOXYLIC ACID 4-TERT-BUTYL ESTER

212650-43-6
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1101987-05-6
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References