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1365272-86-1

N-[1-(4-broMophenyl)cyclopropyl]MethanesulfonaMide synthesis

1synthesis methods
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Yield:1365272-86-1 68%

Reaction Conditions:

Stage #1: methanesulfonyl chloride;1-(4-bromophenyl)-cyclopropylaminewith triethylamine in acetonitrile at 20;Combinatorial reaction / High throughput screening (HTS);Sealed tube;
Stage #2: in acetonitrile at 80; for 2 h;Combinatorial reaction / High throughput screening (HTS);Sealed tube;Sonication;

References:

Bogolubsky, Andrey V.;Moroz, Yurii S.;Mykhailiuk, Pavel K.;Pipko, Sergey E.;Konovets, Anzhelika I.;Sadkova, Irina V.;Tolmachev, Andrey [ACS Combinatorial Science,2014,vol. 16,# 4,p. 192 - 197]