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N-(2-CHLOROBENZYL)PROP-2-EN-1-AMINE synthesis

3synthesis methods
2-Propen-1-amine, N-[(2-chlorophenyl)methylene]-

57966-12-8
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N-(2-CHLOROBENZYL)PROP-2-EN-1-AMINE

103754-08-1
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Yield:103754-08-1 82%

Reaction Conditions:

Stage #1: o-Chlorbenzylidenallylaminwith C21H39NPPd(1-)*C2F3O2(1-);phenylsilane in chloroform-d1 at 40; for 16 h;Glovebox;Sealed tube;
Stage #2: with water in chloroform-d1;Sealed tube;Glovebox;regioselective reaction;

References:

Tafazolian, Hosein;Schmidt, Joseph A.R. [Catalysis science and technology,2016,vol. 6,# 3,p. 685 - 689]

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