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N-(2-Ethoxy-phenyl)-oxalamic acid ethyl ester synthesis

1synthesis methods
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Yield:24439-50-7 82%

Steps:

STARTING MATERIALS

Ethyl N-(2-ethoxyphenyl)oxamate was prepared in 82% yield from o -phenetidine and ethyl oxalyl chloride. The melting point was 67-69°C.

References:

EP593936,1994,A1