N-(2-(Pyridin-2-yl)ethyl)acetamide synthesis
- Product Name:N-(2-(Pyridin-2-yl)ethyl)acetamide
- CAS Number:6304-22-9
- Molecular formula:C9H12N2O
- Molecular Weight:164.2
2706-56-1
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Yield:-
Reaction Conditions:
with pyridine;dmap;acetic anhydride
Steps:
13 N-[2-(2-Pyridinyl)ethyl]acetamide
EXAMPLE 13 N-[2-(2-Pyridinyl)ethyl]acetamide The title compound is prepared by the procedure of Example 12 using 25 g of 2-(2-aminoethyl)pyridine, 22.2 ml of acetic anhydride, 2.57 g of 4-dimethylaminopyridine and 100 ml of pyridine. The residue is purified by column chromatography (silica gel:20% methyl alcohol/ethyl acetate) to give 7.5 g of desired product as a yellow oil. MS:m/z 164 (M+).
References:
US5208247,1993,A
