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ChemicalBook CAS DataBase List N-[4-(2-aminoethyl)phenyl]acetamide

N-[4-(2-aminoethyl)phenyl]acetamide synthesis

3synthesis methods
-

Yield:63630-08-0 80%

Reaction Conditions:

Stage #1: N-[4-(2-azidoethyl)phenyl]acetamidewith triphenylphosphine in tetrahydrofuran at 20; for 15 h;
Stage #2: with water in tetrahydrofuran at 20; for 2 h;

References:

Ishikawa, Fumihiro;Tsumuraya, Takeshi;Fujii, Ikuo [Journal of the American Chemical Society,2009,vol. 131,p. 456 - 457] Location in patent:supporting information; experimental part