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N-(4-Amino-2-methylphenyl)cyclohexanecarboxamide synthesis

2synthesis methods
2719-27-9 Synthesis
Cyclohexanecarboxylic acid chloride

2719-27-9
344 suppliers
$16.00/25mL

N-(4-Amino-2-methylphenyl)cyclohexanecarboxamide

859820-13-6
5 suppliers
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: LiCl / 1-methyl-pyrrolidin-2-one; pyridine / 2 h / 80 °C
2: H2 / palladium on activated carbon / tetrahydrofuran; methanol / 24 h / 40 °C / 2625.26 Torr

References:

Mohmeyer, Nils;Schmidt, Hans-Werner [Chemistry - A European Journal,2007,vol. 13,# 16,p. 4499 - 4509]