N-(4-AMINOPHENYL)-3-METHYLBENZAMIDE synthesis
- Product Name:N-(4-AMINOPHENYL)-3-METHYLBENZAMIDE
- CAS Number:425651-25-8
- Molecular formula:C14H14N2O
- Molecular Weight:226.27
73230-98-5
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425651-25-8
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Yield:425651-25-8 85.2%
Reaction Conditions:
with iron;ammonium chloride in ethanol;water; for 2 h;Reflux;
Steps:
16.2 2. Preparation of 3-methyl-N-(4-aminophenyl)benzamide (11j)
Compound 10j was dissolved in EtOH (20 ml), and an aqueous solution of iron powder (2.5 g) and ammonium chloride (0.53 g, 10 mmol) was added and the reaction was refluxed for 2 hours. Followed by hot filter, collected filtrate spin dry. The resulting solid was dissolved in acetone and the filtrate was collected by filtration and the solution was dried to give compound 11j in 85.2% yield.
References:
CN106699755,2017,A Location in patent:Paragraph 0105; 0285; 0286
99-04-7
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1711-06-4
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100-01-6
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106-50-3
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425651-25-8
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