N-(4-BROMOPHENYL-N-(4-CARBETHOXYPHENYL)AMINE synthesis

7synthesis methods

Product Name:N-(4-BROMOPHENYL-N-(4-CARBETHOXYPHENYL)AMINE
CAS Number:458550-44-2
Molecular formula:C15H14BrNO2
Molecular Weight:320.18

51934-41-9 Synthesis

51934-41-9
285 suppliers
$6.00/5g

586-78-7
1 suppliers
$14.00/5g

N-(4-BROMOPHENYL-N-(4-CARBETHOXYPHENYL)AMINE

458550-44-2
21 suppliers
$154.00/0.25/ G

Yield:458550-44-2 73%

Reaction Conditions:

Stage #1: 4-iodobenzoic acid ethyl esterwith isopropylmagnesium chloride in tetrahydrofuran at -20; for 0.5 h;
Stage #2: para-nitrophenyl bromide in tetrahydrofuran at -20; for 2 h;
Stage #3: with sodium tetrahydroborate;iron(II) chloride in tetrahydrofuran;ethanol at 20; for 2 h;Further stages.;

References:

Sapountzis, Ioannis;Knochel, Paul [Journal of the American Chemical Society,2002,vol. 124,# 32,p. 9390 - 9391]

51934-41-9 Synthesis

51934-41-9
285 suppliers
$6.00/5g

458550-44-2
21 suppliers
$154.00/0.25/ G

References