N-(4-chlorophenyl)pyridine-2-carboxamide synthesis
- Product Name:N-(4-chlorophenyl)pyridine-2-carboxamide
- CAS Number:14547-72-9
- Molecular formula:C12H9ClN2O
- Molecular Weight:232.67
Yield:14547-72-9 866 mg
Reaction Conditions:
Stage #1: pyridine-2-carbonyl chloridewith triethylamine in dichloromethane at 0; for 0.25 h;Inert atmosphere;
Stage #2: 4-chloro-aniline in dichloromethane at 0 - 20; for 2.75 h;Inert atmosphere;
References:
Martinez, Angel Manu;Rodriguez, Nuria;Arrayas, Ramon Gomez;Carretero, Juan C. [Chemical Communications,2014,vol. 50,# 21,p. 2801 - 2803] Location in patent:supporting information
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