N-(4-Fluorobenzyl)-3-Methoxyaniline, 97% synthesis
- Product Name:N-(4-Fluorobenzyl)-3-Methoxyaniline, 97%
- CAS Number:356531-63-0
- Molecular formula:C14H14FNO
- Molecular Weight:231.27
555-03-3
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356531-63-0
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Yield:356531-63-0 71%
Reaction Conditions:
Stage #1: 3-nitroanisolewith hydrogen;palladium on activated charcoal in ethanol at 20; for 1.5 h;
Stage #2: 4-fluorobenzaldehyde in ethanol at 20; for 22.5 h;
Stage #3: with hydrogen;triethylamine;palladium on activated charcoal in ethanol at 20; for 0.166667 h;Further stages.;
References:
Sydnes, Magne O.;Kuse, Masaki;Isobe, Minoru [Tetrahedron,2008,vol. 64,# 27,p. 6406 - 6414]