N-(4-ISOTHIOCYANATO-PHENYL)-ACETAMIDE synthesis
7synthesis methods
- Product Name:N-(4-ISOTHIOCYANATO-PHENYL)-ACETAMIDE
- CAS Number:35008-62-9
- Molecular formula:C9H8N2OS
- Molecular Weight:192.24
Yield:35008-62-9 100%
Reaction Conditions:
Stage #1: carbon disulfide;N-acetyl-p-phenylenediaminewith triethylamine in ethanol at 20;
Stage #2: with dmap;di-tert-butyl dicarbonate in ethanol at 20; for 0.25 h;Further stages.;
References:
Munch, Henrik;Hansen, Jon S.;Pittelkow, Michael;Christensen, J?rn B.;Boas, Ulrik [Tetrahedron Letters,2008,vol. 49,# 19,p. 3117 - 3119]