N-Benzyl-2-bromo-5-fluorobenzamide synthesis
- Product Name:N-Benzyl-2-bromo-5-fluorobenzamide
- CAS Number:951884-18-7
- Molecular formula:C14H11BrFNO
- Molecular Weight:308.15
394-28-5
296 suppliers
$10.00/1g
100-46-9
461 suppliers
$5.00/5G
951884-18-7
17 suppliers
$100.00/1g
Yield:951884-18-7 91%
Reaction Conditions:
Stage #1: 2-Bromo-5-fluorobenzoic acidwith triethylamine;isobutyl chloroformate in dichloromethane; for 0.25 h;Inert atmosphere;Schlenk technique;
Stage #2: benzylamine in dichloromethane at 0;
References:
Liu, Hailong;Han, Weibiao;Li, Chun;Ma, Zhiyong;Li, Ruixiang;Zheng, Xueli;Fu, Haiyan;Chen, Hua [European Journal of Organic Chemistry,2016,vol. 2016,# 2,p. 389 - 393] Location in patent:supporting information