N-Benzyl-4-chloro-N-MethylbenzaMide, 97% synthesis
- Product Name:N-Benzyl-4-chloro-N-MethylbenzaMide, 97%
- CAS Number:137374-28-8
- Molecular formula:C15H14ClNO
- Molecular Weight:259.73
81616-14-0
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C / Inert atmosphere
2.1: 2,2,2-trifluoroethanol; potassium phosphate / 1,4-dioxane / 0.5 h / 125 °C / Sealed tube; Schlenk technique; Inert atmosphere
2.2: 22 h / 125 °C / Sealed tube; Schlenk technique; Inert atmosphere
References:
McPherson, Christopher G.;Caldwell, Nicola;Jamieson, Craig;Simpson, Iain;Watson, Allan J. B. [Organic and Biomolecular Chemistry,2017,vol. 15,# 16,p. 3507 - 3518]
201230-82-2
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1679-18-1
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103-67-3
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137374-28-8
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104-88-1
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19048-85-2
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137374-28-8
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873-76-7
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