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200000-54-0

N-BENZYL-4-FLUOROPHENYLGLYCINE synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: Na2S2O5 / methanol; H2O / 2 h / 35 °C
2: 95 percent / aq. H2O2; K2CO3 / dimethylsulfoxide / 16.5 h / 21 - 35 °C
3: 89 percent / NaOH; H2O / various solvent(s) / 3.5 h / Heating

References:

Davies, Antony J.;Ashwood, Michael S.;Cottrell, Ian F. [Synthetic Communications,2000,vol. 30,# 6,p. 1095 - 1102]