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ChemicalBook CAS DataBase List N-BOC-3-HYDROXY-1,2,3,6-TETRAHYDROPYRIDINE

N-BOC-3-HYDROXY-1,2,3,6-TETRAHYDROPYRIDINE synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: H2O / 6 h / 100 °C
1.2: 66 percent / aq. NaOH / dioxane / 20 °C
2.1: 99 percent / bis(tricyclohexylphosphine)benzylidene Ru(IV) dichloride / CH2Cl2 / 20 °C

References:

Takahata, Hiroki;Suto, Yumiko;Kato, Erina;Yoshimura, Yuichi;Ouchi, Hidekazu [Advanced Synthesis and Catalysis,2007,vol. 349,# 4-5,p. 685 - 693]