ChemicalBook CAS DataBase List N-methoxy-N-methyl-2-nitrobenzamide

N-methoxy-N-methyl-2-nitrobenzamide synthesis

4synthesis methods

Product Name:N-methoxy-N-methyl-2-nitrobenzamide
CAS Number:339221-51-1
Molecular formula:C9H10N2O4
Molecular Weight:210.19

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6638-79-5 Synthesis

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Yield:339221-51-1 95%

Reaction Conditions:

Stage #1: ortho-nitrobenzoic acidwith 4-methyl-morpholine;4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride in tetrahydrofuran at 20; for 1.5 h;
Stage #2: N,O-dimethylhydroxylamine*hydrochloride in tetrahydrofuran at 20; for 8 h;Further stages.;

References:

De Luca;Giacomelli;Taddei [Journal of Organic Chemistry,2001,vol. 66,# 7,p. 2534 - 2537]

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$10.00/10g