N-Methyl-4-Methyl-N-phenylbenzaMide, 97% synthesis
- Product Name:N-Methyl-4-Methyl-N-phenylbenzaMide, 97%
- CAS Number:40669-49-6
- Molecular formula:C15H15NO
- Molecular Weight:225.29
Yield:40669-49-6 95%
Reaction Conditions:
Stage #1: 4-methyl benzoic acidwith oxalyl dichloride;N,N-dimethyl-formamide in dichloromethane at 0 - 20; for 4 h;Inert atmosphere;
Stage #2: N-methyl-N-phenylamine in dichloromethane at 0 - 20;Inert atmosphere;
References:
Shigeno, Masanori;Tohara, Itsuki;Sasaki, Keita;Nozawa-Kumada, Kanako;Kondo, Yoshinori [Organic Letters,2022,vol. 24,# 26,p. 4825 - 4830] Location in patent:supporting information
201230-82-2
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