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98902-12-6

N-METHYL-N-(2-METHYLAMINO-ETHYL)-BENZAMIDE synthesis

3synthesis methods
-

Yield:98902-12-6 31 %

Reaction Conditions:

Stage #1: sym-dimethylethylenediaminewith 9-bora-bicyclo[3.3.1]nonane in tetrahydrofuran;hexane at 20;
Stage #2: 2-Bromobenzoyl chloride in tetrahydrofuran;hexane;

References:

Steimbach, Raphael R.;Herbst-Gervasoni, Corey J.;Lechner, Severin;Stewart, Tracy Murray;Klinke, Glynis;Ridinger, Johannes;Géraldy, Magalie N. E.;Tihanyi, Gergely;Foley, Jackson R.;Uhrig, Ulrike;Kuster, Bernhard;Poschet, Gernot;Casero, Robert A.;Médard, Guillaume;Oehme, Ina;Christianson, David W.;Gunkel, Nikolas;Miller, Aubry K. [Journal of the American Chemical Society,2022,vol. 144,# 41,p. 18861 - 18875] Location in patent:supporting information

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