ChemicalBook CAS DataBase List N-(MORPHOLIN-2-YLMETHYL)ACETAMIDE

N-(MORPHOLIN-2-YLMETHYL)ACETAMIDE synthesis

3synthesis methods

Product Name:N-(MORPHOLIN-2-YLMETHYL)ACETAMIDE
CAS Number:112913-95-8
Molecular formula:C7H14N2O2
Molecular Weight:158.2

Acetamide, N-[[4-(phenylmethyl)-2-morpholinyl]methyl]-

112913-96-9
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112913-95-8
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Yield:112913-95-8 100%

Reaction Conditions:

palladium-carbon in ethyl acetate;

Steps:

P.5.f f

f 2-(N-Acetylaminomethyl)morpholine STR27 In a solution of 2-(N-acetylaminomethyl)-4-benzylmorpholine (20 g, 80.7 mmol) in ethanol-acetic acid (20/1, 210 ml) was suspended 2.0 g of 10% palladium-carbon and the mixture was stirred at 60° C. under hydrogen stream for 22 hours. The reaction mixture was filtered with Celite, the solvent was distilled off from the filtrate under reduced pressure to give crude 2-(N-acetylaminomethyl)morpholine (15.62 g). Yield=100%. This compound was used for the subsequent reaction without purification.

References:

US5736550,1998,A

40987-25-5
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112913-95-8
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$155.00/100mg

References

110859-48-8 Synthesis

2-(4-BENZYL-MORPHOLIN-2-YLMETHYL)-ISOINDOLE-1,3-DIONE

110859-48-8
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$45.00/100mg

112913-95-8
19 suppliers
$155.00/100mg

References