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ChemicalBook CAS DataBase List N,N-bis(2-chloroethyl)-4-methoxyBenzenemethanamine
91561-99-8

N,N-bis(2-chloroethyl)-4-methoxyBenzenemethanamine synthesis

2synthesis methods
-

Yield:91561-99-8 75%

Steps:

101

4-Methoxybenzyl-bis-(2-chloro-ethyl)-amine was prepared according to the general method as outlined in example 83. Starting from 4-Methoxy-benzyl diethanolamine (10 g, 44 mmol). Yield 10 g (75 %); yellow solid mp 55 C; MS: 263.1 (M+H)+.

References:

EP970046,2003,B1 Location in patent:Page 53