N,N-bis(2-hydroxyethyl)octanamide synthesis
1synthesis methods
- Product Name:N,N-bis(2-hydroxyethyl)octanamide
- CAS Number:3077-30-3
- Molecular formula:C12H25NO3
- Molecular Weight:231.33
Yield:-
Reaction Conditions:
Stage #1:Octanoic acid;2,2'-iminobis[ethanol] with benzotriazol-1-ol;triethylamine in dichloromethane for 0.25 h;Cooling with ice;
Stage #2: with 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane at 20;Cooling with ice;
References:
Xun, Miao-Miao;Zhang, Xue-Chao;Zhang, Ji;Jiang, Qian-Qian;Yi, Wen-Jing;Zhu, Wen;Yu, Xiao-Qi [Organic and Biomolecular Chemistry,2013,vol. 11,# 7,p. 1242 - 1250]