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ChemicalBook CAS DataBase List N,N-diallyl-1-phenylethylamine

N,N-diallyl-1-phenylethylamine synthesis

4synthesis methods
-

Yield:92499-04-2 86%

Reaction Conditions:

Stage #1: acetophenone;diallylaminewith titanium tetrachloride in dichloromethane at 20; for 3 h;
Stage #2: with sodium cyanoborohydride in methanol;dichloromethane at 20; for 1 h;

References:

Rahman, Obaidur;Kihlberg, Tor;Langstroem, Bengt [Organic and Biomolecular Chemistry,2004,vol. 2,# 11,p. 1612 - 1616]