ChemicalBook CAS DataBase List (N,N-DIMETHYLAMINO)DIMETHYLCHLOROSILANE

(N,N-DIMETHYLAMINO)DIMETHYLCHLOROSILANE synthesis

6synthesis methods

Product Name:(N,N-DIMETHYLAMINO)DIMETHYLCHLOROSILANE
CAS Number:18209-60-4
Molecular formula:C4H12ClNSi
Molecular Weight:137.68

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Yield:18209-60-4 97%

Reaction Conditions:

at 20; for 14 h;

Steps:

5 Reference Example 5

14.3 g (97.9 mmol) of bis (dimethylamino) dimethylsilane was added to 12.6 g (97.9 mmol) of dichlorodimethylsilane and the mixture was stirred at room temperature for 14 hours. A small amount of the insoluble matter formed was filtered off using a glass filter (G4) to obtain 26.3 g of chloro (dimethylamino) dimethylsilane as a colorless liquid. Yield 97%

References:

JP2016/147819,2016,A Location in patent:Paragraph 0075

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