N,N-DIMETHYLOCTYLAMINE-N-OXIDE synthesis

Yield: 98%

Reaction Conditions:

with dihydrogen peroxide;benzonitrile;Mg-Al-O-t-Bu HT (Catalyst B) in methanol;water at 65; for 0.5 h;Product distribution / selectivity;

Steps:

18
Oxidation of various tertiary amines using catalyst B was carried out following the procedure as in example 2 and the results are given in Table 2.

References:

Council of Scientific and Industrial Research EP1348692, 2003, A1 Location in patent:Page/Page column 7