N-tert-Butyl-2-chloroisonicotinamide synthesis
- Product Name:N-tert-Butyl-2-chloroisonicotinamide
- CAS Number:588694-28-4
- Molecular formula:C10H13ClN2O
- Molecular Weight:212.68
6313-54-8
417 suppliers
$8.00/5g
75-64-9
420 suppliers
$10.00/10g
588694-28-4
15 suppliers
$131.00/1g
Yield:588694-28-4 56%
Reaction Conditions:
Stage #1: 2-chloroisonicotinic acid,with thionyl chloride for 2 h;Heating;
Stage #2: tert-butylamine in dichloromethane at 20; for 20 h;Further stages.;
References:
Hawad, Ha?an;Bayh, Omar;Hoarau, Christophe;Trécourt, Francois;Quéguiner, Guy;Marsais, Francis [Tetrahedron,2008,vol. 64,# 14,p. 3236 - 3245]
6313-54-8
417 suppliers
$8.00/5g
588694-28-4
15 suppliers
$131.00/1g
65287-34-5
94 suppliers
$50.75/1g
75-64-9
420 suppliers
$10.00/10g
588694-28-4
15 suppliers
$131.00/1g